3

MASS2 100 1 5010315850100150mzIR100501 4000 'H NMR 300 MHz1 V 3000 2000 1000 Wavenumber (cm-| )3.53.02.52.0151.0ppm"CIDEPT NMR 75.5 MHz Dret 90 Dt_ks20018...

Question

MASS2 100 1 5010315850100150mzIR100501 4000 'H NMR 300 MHz1 V 3000 2000 1000 Wavenumber (cm-| )3.53.02.52.0151.0ppm"CIDEPT NMR 75.5 MHz Dret 90 Dt_ks20018016014012010080ppm

MASS 2 100 1 50 103 158 50 100 150 mz IR 100 50 1 4000 'H NMR 300 MHz 1 V 3000 2000 1000 Wavenumber (cm-| ) 3.5 3.0 2.5 2.0 15 1.0 ppm "CIDEPT NMR 75.5 MHz Dret 90 Dt_ks 200 180 160 140 120 100 80 ppm



Answers

Match the $^{13}$C NMR data to the appropriate structure.
Spectrum [1]: signals at 14, 22, 27, 34,181 ppm
Spectrum [2]: signals at 27, 39, 186 ppm
Spectrum [3]: signals at 22, 26, 43, 180 ppm

Hillary won today were doing Chapter fourteen point seventy eight and it's from tells us that phosphorus p thirty one it has on mass number so absorbs in anymore. And it tells us that the fosters nuclear actually behaved very similar to pro trump protons in the NMR spectroscopy. So with this in mind, explain why when we do a proton anymore of this molecule here we get two double its one at one point five ppm and one of three point seven p. P. M. Ore. The question is telling us that phosphorus but hey similarly two protons in and tomorrow we know that protons that they can be slated by neighboring proton. So if a fast wrist behaves like a proton than it should be, we can determine that it's gonna split neighboring protons off. For example, the three protons in this metal group, our neighboring one phosphorus. So then, using the n plus one rule, this foster's can act as a neighboring proton. So we have a neighboring of one plus one to give us too. So we have three protons that represents a doublet and all we have to a cool and proton types here. These are both the same. They're all bound to three. This carbon is about three protons of one option from each side. So no, they're equivalent. Well, these three protons also neighboring one fosters. So using the endless wonderful again we'LL say that these three protons are neighboring is one phosphorus who have neighboring one to give us a doublet, which is here. You know that these three are gonna have a more downfield shifted value because of proximity to this auction. Adam here, compared to this method group should have the one points five value up here.

Hi, everyone. One age, the normal spectrum or being seen shores. Oh, sing leg I Hi Year Delta off some 0.2 ppm. Big because they're not because the benzene dream. Yeah, not only consist, stop consists off. Alternative single and double bonds, Single can and double box. Yeah, Trump, but unsold. It has a ring strain A ring strain. Do you do? Hey, exact journal. Close structure. Clothes struck Chip. On the other hand, on the other hand, Sunday Other hand 13 Butor dying Butor dying So although it is conjugated so those it is conjugated shots Lower frequency peak. Okay, free quinces. I Delta fire you comma the top 5.1 and 6.3 PM You hear? Since it has open structure open structure I am doing strain is absent on the ring strain is upset of sand, right? Secondly, aromatic compounds A I don't My big compound A shows mass spectrum pig spectrum peak. I am I said 104 Therefore the compound heads molecular formula. See a day agent check. Secondly, the 11 tell analysis off A unless it's off a indicates you know for example element the percentage then atomic ratio Dane Sim Blessed atomic ratio 11 days Carbon hydrogen 92.3 This is 7.7%. So this will come at the 7.69 This is 7.7 simplistic comic racial point people Line, this is one so whole numbers that is in tow Aid. Get eight toe eight again aid and therefore no their fault. The formula of the components the comm Bondi's combined aids C h h aid Angry restructure is structure off is as follows. So structure up Is this true? C h that we want ch two So this sort a compound a Now this component a combined a under rumination Yes. Cambone be Be so sure. Okay. C h double one ch teau less We are too. So this is basically sliding. So one robin is I didn't do this against the first Carbon and other women is ready to stake in carbon ain't will get well, kids ch br ch trupia. So this is what they compounded. Gate nineteen's one Bram Oh, one fan Ill. Yeah. Uh, we can greatly this also that this one to diagram Oh, on to die a brahma one final We think the thing So this is combined A and this is combined The okay


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