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A) How would you carry out the following synthesis? You may use any reagent(s) you wish.b) A standard synthetic sequence for building a six-membered cyclic ketone o...

Question

A) How would you carry out the following synthesis? You may use any reagent(s) you wish.b) A standard synthetic sequence for building a six-membered cyclic ketone onto an existing aromatic ring is shown in outline as follows. Specify the reagents necessary for each step:OHOH

a) How would you carry out the following synthesis? You may use any reagent(s) you wish. b) A standard synthetic sequence for building a six-membered cyclic ketone onto an existing aromatic ring is shown in outline as follows. Specify the reagents necessary for each step: OH OH



Answers

Synthesis of Amines How would you prepare the following substances from 1-butanol? (a) Butylamine (b) Dibutylamine (c) Propylamine (d) Pentylamine (e) $N, N$ -Dimethylbutylamine (f) Propene

Hillary want whoever during chapter 23 poems 60 forints from ass to drug to different hallow ketones are conformed a bi intra molecular calculation reaction and be synthesized a using issue acidic as your servicer Solis Servan s o the service. The hallow key tone. So we didn't just start with a very simple one. It's one Brahmin. Then we see that we have to add this entire our group. But we already have intellectual found here. So we need to make this carbon good fall. So that way we can do is make that into a cranium so we can add and g b are so green arid regions. And then this counter number carbons and you want to answer We have 123 for five, and then six carbon. And then we have these six here on the side of the sixth car. That was not a blown me so first thing first What I react Thes tool. This is the car Bannon's do a new cliff look attack of this position. So what we're gonna be left with is something that looks like this. And now if I add in some sort of strong base So I'm a dockside deep. Only the alpha proton here deformity estimate carbonite and witching goes through an essence who stepwise essence to a neutral flick Attack at this carbon Electra filler. Carbon here to kick off roaming to now form the final product like this. So this is one way in no way is that you can actually make pull through these carbon nuclear Philip by having both the mounds of green, your region so and DVR and junior. And then you're going to react that with now your key tone. But now I'm gonna have to heroes. So then you're gonna have to nickel files attacking the carbon with your tool. You're leaving groups. So then right away, in one step, you'll get your final product. This reaction will be very messy. Go Wouldn't really recommend Doing this in the lab is because you are very minimal control about what else can go on this reaction. But is that to ask possibilities form for using the conditions provided in the question of Halki tone But apart being us to do from the cereal asio acid acidic acid S s s s so sorry. From where asio acidic acid um we start from the estrogen being thiss, and now we have a strong base. Sorry, it's oxide and they weren't at our electro file. There's even be the carbons that we need to answer all of these carbons here. We'll see home of drawing it. That kind of little resembles the shape that I want. So it is easier to count carbons that way. So after one equivalence of this reaction, we'll have reacted one of these Elektra files. So we make our man, and I'll hit one of these electoral Filic carbon centers to form this. And then if I reacted with another equivalent of space sort of meth oxide, you make deep only the other second. But Proton proton here to form the carbon in which can then go threats into backside attack to give us this product here like this. And now, if I at an acidic water and heat, you get spontaneous Deke remarks, elation and hide dialysis off our Esther. Just leave our Qi Tian plus years

Okay, so rest create the following products from the given Solomon zero. And in the first one we got three carbon alcohol super panel and we want to create the structure so we can add Berman an anti edition across an arcane by using BR two with some non equity solvent. But we need to turn the alcohol into Naquin or military structure just into our keen and we can do this to dehydrate extraction by reacting, reacting the alcohol with a strong acid and heat. The auction's going to department the acid and um, we call it the base of the assets, going to grab parts on before the most evil cane in this case is from a matter but to formula kino right there and if we react the structure now with the art, so and a non equity solvent, it's going to add burning and anti edition meaning ones in the front and once in the back And the next one is a purple. All we're going to create an ester. Okay, so I'm gonna use um um you want to use the oxidative cleavage direction of AKIN's. So I want to get Naquin from the alcohol. And he had reacting this with sulfuric acid for some of the strong acid and heat and they're reacting the a keen with 23 and this is under um a um this is a reduction reaction. So this is gonna be a zinc and water and really it's just going to prevent the hydrogen from becoming Carlos of acids. So if we reacted this with A three and then a stronger oxidizing agent, it would turn the hydrogen of the AKIN into a corrosive acid. But what's gonna happen here is that it's not clear that gold bond, it's going to add a key tune to this carbon and um burning it formaldehyde on that carbon. So we get to our hurts. And um so I'm gonna react. I want to turn to keep the out to hide into carrasco acid, Someone oxidize it with, um, with potassium permanganate. So now we have caramel, so acid and we can get an ester through fisher justification. So you want to add, we want to react this with a two carbon alcohol and while the loss of water and this is also done in the presence of nasa catalyst with heat, a blue to get water as a side product. And also the asked back to, so really the goal of oxidative cleavage was we couldn't really, we couldn't really get a carb also asset here because we would have a three carbon corrosive acid and it would match the product. So we had to break Basically one carbon off. So that was where the purpose of oxidative cleavage. And then from there we could use fish stratification to get the Esther

Preparation of different alcohols using Did not reaction first one to penned an old to general 12345 So it is here. It's a secondary alcohol. So you're starting with you is going to be and I'll be heard him See Expo and see It's three MTV are so all the heads will give a second of alcohol already heights. Thank you Sink Country alcohol Second companies. One you can order Mhm one mutant or it's a primary alcohol which can be obtained from for my head. Yes, No All my head with the big not reusing MDBR That's let's see h four. So they let's come. Bonus one tonight. Cyclo hexane all slate blue. Thanks and all will be help. So you seem all too see 685 Find who A year. It's a tertiary alcohol so totally alcohol can be prepared from the corresponding T tones like the fictional Let's United Migration Broadway MDBR next to diagnose metal our Dia Final methanol. So we have see things that's fine or it's year. This can be obtained from my name is Joe Mhm. I called meat s camp and two more games off. We you know in the nation WalMart, so we can help each c W ball ball. Well, ch three that's 36 and 12 NTV are two modes of it.


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